Oligocellulose from acid hydrolysis: A revisit

نویسندگان

چکیده

The classical method of producing cellulose oligomers through hydrolysis microcrystalline (MCC) in phosphoric acid has been re-examined. Hydrolysis products are fractionated by precipitation to yield two types with different average degrees polymerization (DP). number- and weight-averaged molecular weights the lower DP fraction 1339 g/mol 1388 respectively, corresponding a polydispersity index 1.04. oligomer forms type-II crystal, can be dissolved both alkaline aqueous solutions dimethyl sulfoxide. X-ray neutron small angle scattering solution described as rigid slabs.

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ژورنال

عنوان ژورنال: Applied Surface Science

سال: 2021

ISSN: ['1873-5584', '0169-4332']

DOI: https://doi.org/10.1016/j.apsusc.2020.147783